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Last Updated Thursday, 20 October 2011 17:10
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Laboratory of Microanalysis


Head of the Laboratory: Ph. D. Anastassiya G. Buyanovskaya.

Phone

7-499-135-76-03

7-499-135-93-90

E-mail

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The Laboratory of Microanalysis at the A.N. Nesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences, is one of the leading analytical laboratories in the Russian Federation. The Laboratory is specialized in elemental analysis of organic and organoelement compounds, polymers, and other materials based on them.

Professional skills of the Laboratory staff and the use of modern analytical techniques provide the possibility of analyzing thousands of multi-element samples per year.


The Laboratory of Microanalysis offers the following methods for quantitative analysis of elements constituting organoelement compounds and materials:

  • Automatic CHN(O, S) analysis
  • Classical elemental microanalysis
      • Modified Pregl determination of carbon and hydrogen, ash-forming elements (B, P, Si, metals), sulfur, halogens (Cl, Br, I)
      • Manual simultaneous determination up to five elements using one sample
      • Modified Duma determination of nitrogen
      • Schoniger determination of sulfur and halogens (F, Cl, Br)
  • Special analytical methods
    • Analysis of B-, F-, P-, Si-, Os-, Ru-containing and other organometallic compounds
    • Analysis of metallosiloxanes
    • Analysis of hardly burnt samples (graphites, carboranes, fullerenes)
    • Analysis of liquid, volatile, labile compounds
    • Ultramicroanalysis
  • Decomposition methods
  • Combustion in an oxygen stream
  • Combustion in an oxygen-filled flask
  • Decomposition in presence of metal oxides
  • Alkaline fusion
    • Acid digestion
    • Microwave digestion
    • Finish techniques
    • Express-gravimetry
    • Titrimetry
    • Spectrophotometry
    • Polarography
    • Coulometry
    • Ion chromatography
    • Atomic absorption
  • Nondestructive X-ray fluorescence analysis


Special equipment, alternative methods, and professional skills of the Laboratory staff guarantee:

fast order performance (23 days) and accuracy and high reliability of results.


Mailing Address: Laboratory of Microanalysis, A. N. Nesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences, 28 ul. Vavilova, 117813 Moscow, Russian Federation.



Laboratory of Homolytic Reactions of Organoelement Compounds


Head of the Laboratory: Dr.Sc. Konstantin A. Kochetkov

Phone

7-499-135-5033

E-mail

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The Analytical Exploration Unit of the GREOS Laboratory, A.N.Nesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences, is specialized in performing GLC and HPLC analyses of organic and organoelement compounds and materials based on them (e.g., trace analyses of biological samples for dicarboxylic and fatty acids, analysis of enantiomeric amino acids, etc.). New analytical procedures are developed if necessary.

Professional skills of the Analytical Exploration Unit staff guarantee fast order performance and the accuracy and high reliability of results.

Mailing Address:
Dr.Sc. Konstantin A. Kochetkov, GREOS Laboratory, A.N.Nesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences, 28 st. Vavilova, 119991 Moscow, Russian Federation.



Laboratory for Filled Polymer Systems


Head of the laboratory: Dr.Sc. Alexander P. Krasnov

Phone

7-499-135-6374

E-mail

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Determination of physicomechanical indices (hardness, impact strength, etc.), frictional performances, properties of the materials’ surface (wetting angle, microhardness).



Laboratory for Polymer Structural Research

Head of the laboratory: Dr.Sc. Alexander I. Pertsin

Phone

7-499-135-6385

E-mail

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For our colleagues from INEOS, we offer powder diffraction - a useful tool to distinguish and characterize small-molecule organic and organoelement compounds.



Laboratory for X-Ray Diffraction Studies - X-Ray Structural Centre (XRSC)

Head of the laboratory: Corresponding Member of the Russian Academy of Sciences, Prof., Dr. Sc. Mikhail Yu. Antipin

Phones

7-499-135-9215

7-499-135-9271

Fax:

7-499-135-5085

E-mail

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Contact the XRSC Director at:
Mikhail Yu. Antipin, X-Ray Structural Centre Institute of Organoelement Compounds, 28 Vavilov St., B-334, Moscow, 119991, Russia


X-Ray Structural Centre (XRSC) - one of the most efficient X-ray structural laboratories in the world - carries out as well on a commercial basis X-ray structural analysis of crystals of virtually all classes of compounds, including those highly unstable, liquid or even gaseous at ambient temperature (excluding proteins and high polymers).

If you send a small crystal sample (about 0.5 mm) or a 10-15 mm long capillary filled with a liquid, we will provide you with a wealth of fully objective information on empirical formula, molecular structure, accurate bond lengths and angles, molecular conformation and absolute configuration, peculiarities of crystal packing, and/or optionally molecular mechanics and quantum chemistry analysis of the structure.

Best experimental equipment, extensive computing and computer graphics facilities, and above all highly skilled personnel with many years of experience in the field are the guarantees of prompt service (several days for urgent orders), absolute reliability, and highest possible accuracy of the results.

Our Centre is capable of fulfilling all your X-ray crystallography needs at great savings of time and money. The world has become quite small and you'll have no problems contacting us. Just give it a try - send a few crystals of your sample by express mail, e.g. DHL or TNT, and in almost no time you'll receive the molecular structure by fax or E-mail. Best of all - your first crystal structure is free! And you will be surprised by our regular prices that are significantly lower than anywhere else. We guarantee full confidentiality and will have no claims for co-authorship or any other rights to the information related to or obtained by the XRSC as a part of its commercial activities.

The XRSC is also an official affiliation Centre for distribution of the current version of the Cambridge Structural Database in Russia and former USSR countries. At present, new CSD version is distributed by XRSC at 55 institutions and organizations.


Center for Sophisticated Instrument Facilities  Center for Physical Methods of Substances Studies (FIMIS)

A common-access sophisticated instrumentation facility

Director of FIMIS

Academician of RAS, Professor  Alexei R. Khokhlov
phone: 7-499-135-79-10
e-mail: This e-mail address is being protected from spambots. You need JavaScript enabled to view it , This e-mail address is being protected from spambots. You need JavaScript enabled to view it

Deputy Director of FIMIS

Prof. Boris V. Lokshin
phone:  7-499-135-65-01
fax: 7-499-135-5085
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The Center for Physical Methods of Substances Studies (FIMIS) is a non-profit enterprise. It was established in order to offer experimental studies service for research projects supported by the Russian Foundation for Basic Research (RFBR) grants. FIMIS was founded by the Institute of Organoelement Compounds of Russian Academy of Sciences (INEOS RAS) and by the Institute of Chemical Physics of RAS (ICP RAS). The financial support for the Center is provided by RFBR.

Due to a support from RFBR as well as from the founder Institutes, modern equipment for experimental studies of materials by physical methods was recently purchased. This equipment was installed in the corresponding FIMIS Departments. The Departments offer their service not only for their host institutions, but also for all holders of RFBR grants.

On special agreements, FIMIS may perform physical studies for any institutions and enterprises not holding RFBR grants, in accordance with the specialisation of its Departments.

FIMIS invites all RFBR grantees to a fruitful co-operation.

Postal address:

Center for Physical Studies of Material Structures (FIMIS), Institute of Organoelement Compounds (INEOS) RAS, 28 Vavilov street, V-334, GSP-1, Moscow 119991, Russia.